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Table 5 Results of the hydrothermal stability measurement, fibre assessment and amino acid analysis of the nine selected micro samples compared with reference values of new reference materials (standard deviations in parenthesis)

From: Assessing the condition of the Domesday Books from the visual to the molecular

Sample no.

Tf (°C)

Ts (°C)

Dam. fibres (%)

Tyr

His

Hyl

Lys

Arg

Suma

LD 1v

39.6

53.9

72

0.32

0.77

0.41

2.34

4.34

8.18

GD 2v

48.1

60.0

66

0.42

0.87

0.40

2.52

4.88

9.09

LD 109v

50.3

60.8

67

0.58

0.49

0.44

2.23

4.99

8.73

LD 183v

43.3

49.6

71

0.41

0.71

0.40

2.34

4.77

8.63

GD 202v

48.2

54.8

71

0.40

0.72

0.37

2.26

4.85

8.6

GD 203v

44.3

58.6

79

0.32

0.58

0.40

2.03

4.57

7.90

GD 382v

b

b

100

0.41

0.76

0.45

2.43

4.68

8.73

LD 412v

35.8

61.0

56

0.82

1.49

0.34

2.94

4.62

10.21

LD 449rc

         

New reference

 

≈ 60

≤ 30%

0.41 (0.03)

1.31 (0.03)

0.72 (0.05)

2.62 (0.05)

5.04 (0.06)

10.10 (0.04)

  1. aSum = Σ Tyr, His, Hyl, Lys, Arg
  2. bDissolves by contact with water
  3. cSample too small for microanalysis except for X-ray diffraction analysis