From: Colouring of Pacific barkcloths: identification of the brown, red and yellow colourants used in the decoration of historic Pacific barkcloths
Time (min)
Water (%)
Acetonitrile (%)
5% H3PO4 (%)
HPLC gradient 1
0
68
30
2
25
98
30.1
35
HPLC gradient 2
85
10
5
95
25.1