From: Low-radiation dose XRF excited by MeV protons for cultural heritage samples
 | Thick standard sample for LOD evaluation | Simulated cultural heritage sample | ||||
---|---|---|---|---|---|---|
Sample number | #1 | #2 | #3 | #4 | #5 | #6 |
Compound or pigment | Copper(II) sulfate pentahydrate (CuSO4·5H2O) | Azurite (Cu3(CO3)2(OH)2) | Smalt (SiO2·K2O·CoO) | Azurite + smalt | ||
Base binding medium | Gelatin (C65H102N18O21) | |||||
Support material | (None) | 4.5Â mg/cm2-thick Japanese hemp paper | ||||
Preparation method | Homogenization and pelletization | Painting on paper support and drying | ||||
Element of interest | Cu | Cu | Co | Cu and Co | ||
Mass concentration | 0Â ppm | 1000Â ppm | 10,000Â ppm | 28%a | 3.9%a | Cu 14%a Co 2.0%a |
Thickness | ≈ 7 mm (cylindrical pellet height) | 140 µmb | 340 µmb | 190 µmb |