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Table 3 A critical comparison of the tested methods of sample preparation for FTIR analysis

From: Methodology for infrared spectroscopy analysis of sandwich multilayer samples of historical materials

Method of sample preparation

Cross-section compactness

No sample contamination

Archiving

Laboriousness

Evaluation

Barrier methods

Silicate (Liquid glass)

+

Limited

+

+

2

Dispersion of vinyl acetate

+

-

+

+

5

Cyclododecane - melt

-

Limited

Limited

+

4

Cyclododecane - solution

+

Limited

+

+

2

Carbon coating

+

+

+

-

1

Gold sputtering

+

+

+

-

1

KBr pellet

Sample cut askew

+

+

Limited

-

1

Sample grind down in pellet

+

+

Limited

-

1

Twice moulded sample

+

+

Limited

-

1

  1. Mark "1" belongs to the best, mark "5" to the worst one.
  2. +… Method meets the requirement
  3. - … Method does not meet the requirement
  4. Limited … The requirement is only partially met
  5. The methods are evaluated with respect to analysis accuracy.